After being rinsed with deionized water, they were soaked in ethanol for 30 min, rinsed with deionized water again, and dried in the oven at 50°C for 30 min. Then, an Au film whose thickness was about 50 nm was deposited on
the substrate. High-purity Zn powders (99.999%) were placed in the quartz boat, and then, the quartz boat was put in the center of the tube furnace. The substrate was placed about 5 cm away from the quartz boat. Previous to the growth, the tube furnace was pumped to 5 Pa. Subsequently, the temperature of tube furnace was raised to 650°C for 30 min under the protection of Ar (120 sccm). Then, O2 (80 sccm) was introduced into the furnace. The growth lasted for 40 min. Then, the whose system was cooled to 25°C. After that, the ZnO C188-9 in vivo nanorod arrays were grown on the surface of the stainless steel mesh. find more Lastly, the as-prepared sample was stored in the dark room for 2 weeks before it was measured. selleck inhibitor The surface morphology of the ZnO nanorod was studied using scanning electron microscope (SEM, Hitachi S4700, Chiyoda-ku, Japan). The phase identification of the ZnO nanorod was carried out with X-ray diffraction (XRD, Cu Kα). The contact angles on the as-grown sample were measured by contact angle meter (DSA100, KRÜSS, Hamburg, Germany).
Results and discussion Figure 1 indicates the SEM images of the as-grown sample. As shown in Figure 1a, the surface of stainless steel mesh was covered uniformly with the ZnO nanorod arrays.
It can be found that the highly uniform and densely packed ZnO nanorods were grown on a stainless steel wire; the average diameter of the ZnO nanorod is about 85 nm (Figure 1b,c). Figure 1d shows the cross-sectional view of the ZnO nanorod arrays. We can found that the ZnO nanorod arrays are almost vertical to the surface of the stainless steel wire, and the heights are about 4 μm. Figure 2 shows the XRD pattern of the ZnO nanorod arrays coated on stainless steel mesh. Three peaks (100), (002), and (101) can be deduced. The intensities of (100) and (101) peaks are much lower than the (002) peak. Dehydratase This indicates that the as-grown sample is a polycrystalline wurtzite ZnO and along  direction. Figure 1 SEM images of the as-grown ZnO nanorod arrays on the stainless steel mesh. (a) Large-area view of the coated mesh, (b) top images of the ZnO nanorod arrays on a stainless steel wire, (c) high-magnification ZnO nanorod arrays on a stainless steel wire, and (d) SEM side views of the ZnO nanorod arrays with height about 4 μm. Figure 2 XRD patterns of the as-grown sample. The slow-growing planes usually have low surface free energy . The growth rates of the ZnO crystal were reported to be [−100] > [−101] >  ≈ [00–1] . Figure 2 shows that the surface of the ZnO nanorod is the (001) plane.